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GREEN SOLVENT ASSISTED UV-SPECTROPHOTOMETRIC METHOD FOR ESTIMATION OF PIROXICAM IN BULK AND TABLET DOSAGE FORM (Record no. 131746)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 01472nam a2200133 4500 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 250623b |||||||| |||| 00| 0 eng d |
| 100 ## - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Vikas Chauhan |
| 245 ## - TITLE STATEMENT | |
| Title | GREEN SOLVENT ASSISTED UV-SPECTROPHOTOMETRIC METHOD FOR ESTIMATION OF PIROXICAM IN BULK AND TABLET DOSAGE FORM |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | P 74-82 |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. biblio.abstract | A precise, simple, economical and accurate UV spectroscopy-assisted method has been developed to estimate piroxicam (PRXM) in pure API and tablet dosage form. The absorbance maxima of PRXM were found at 357nm λmax using water (H2O) and methanol (MeOH) in a ratio of 40:60 V/V as a solvent. For concentrations between 2 μg mL-1 - 12 μg mL-1, the procedure adheres to Beer's law with an R2 value of 0.9992, the linearity was found in the calibration curve between absorbance and concentration in accordance with the line equation y=0.0508x+0.0085. The LOD and LOQ were found to be 0.90 µg mL-1 and 2.74 µg mL-1, respectively. The proposed method was effectively used to calculate PRXM in bulk drug and pharmaceutical formulations without common excipient influence and the % RSD was found 0.79, with an average % recovery of 99.57 %. The developed method was validated in accordance with ICH Q2 (R1) guidelines. |
| 654 ## - SUBJECT ADDED ENTRY--FACETED TOPICAL TERMS | |
| Subject | <a href="Piroxicam (PRXM)">Piroxicam (PRXM)</a> |
| -- | <a href="analytical method">analytical method</a> |
| -- | <a href="UV spectrophotometry">UV spectrophotometry</a> |
| -- | <a href="validation">validation</a> |
| -- | <a href="tablet dosage form">tablet dosage form</a> |
| 773 0# - HOST ITEM ENTRY | |
| Host Biblionumber | 125265 |
| Host Itemnumber | 112316 |
| Place, publisher, and date of publication | Mumbai Indian Drugs Manufacturer's Association |
| Title | Indian Drugs |
| International Standard Serial Number | 0019-462X |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Koha item type | Journal Article |
| Withdrawn status | Lost status | Source of classification or shelving scheme | Damaged status | Not for loan | Location (home branch) | Sublocation or collection (holding branch) | Date acquired | Koha issues (times borrowed) | Piece designation (barcode) | Koha date last seen | Price effective from | Koha item type |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Dewey Decimal Classification | SNDT Juhu | SNDT Juhu | 23/06/2025 | JP599.8 | 23/06/2025 | 23/06/2025 | Journal Article |